Fine bubbles in the edge after the autoclave process
Film temperature too high after pressure release
Cooling stage in the autoclave process must be lengthened until max. glass temperature of 40°C (104°F) is reached, then release pressure and immediately open the door. Check the glass temperature with measuring instrument; calibrate measuring sensor/autoclave if necessary
Larger bubbles in the edge/bubbles limited locally
Poor edge seal in pre-laminate
Improve by raising temperature during pre-lamination
Film at the two longitudinal edges too wet
Store rolls at 25 – 30% rel. humidity Check climate setting in processing room prüfen
Creases in the film due to incorrect lay-up
Processing room/ personnel training
Film pulled out prior to cutting (too thin or missing)
Processing room/ personnel training
Plies not correctly placed together or poorly bent
Ensure accurate match Check bending tolerance
Inserted objects too thick/not suitable for assembly
Check objects Increase PVB film thickness
Autoclave process not optimal (too low/too high pressure increase in comparison with temperature; pressure release when temperature is too high)
Optimise process acc. to recommendation
Supporting material is too soft
Use harder supporting materials, e.g. Teflon strips
Too little/too much detergent in the washing water (dirt/cutting oils as residue on the glass)
Check dryness of washed glass
Check washing brush setting; renew brushes if necessary
Check film moisture/climate in the lay-up room; check glass planeness FTG/HSG with straight edge
Check bending tolerance of glass
Check coating compatibility of glass to PVB
Check pre-laminate conditions/ autoclave parameters; see 1.1
For screen printing on glass: check compatibility/ level of printing
2. DEFECTS AT HIGH TEMPERATURES
2.1 BOIL TEST 2H/100°C (212°F)
Fault
Cause
Optimization
Bubbles in Laminated Safety Glass
Wrinkles in PVB
Change processing conditions; see 1.1
Faulty glass alignment/glass bending tolerances too high
Check tolerances Optimise glass alignment
Glass temperature too high when laminated
Check washing conditions; see 1.3
Pre-laminate conditions wrong/too early edge seal/roll gap too wide
see 1.1 and 1.2
Inserted objects too thick/ not suitable
Check objects; see 1.1
Glass coating not compatible with PVB film
Check compatibility
Moisture content in PVB too high
Check climate setting/ lay-up room
2.2 BAKE TEST
If bubbles arise at temperatures below 130°C (266°F) then the moisture content in the laminated safety glass is too high or pre-laminate deairing is poor. However, there can also be other causes.
3. MOISTURE CONTENT
3.1 MOISTURE CONTENT
Fault
Cause
Optimization
Moisture in Laminated Safety Glass too high/too low
Film stored too humid/ too dry
Check storage conditions/ packaging
Climate in the lay-up room
Check climate (should be approx. 25 – 30% rel. humidity)
Washed glass is not dry
Check washing machine (washing water temperature, drier, line speed)
Storage time of pre-laminate is too long
Shorten storage time
Film wrongly stretched (windscreen)
Check stretch conditions Use PVB film with higher initial moisture
Moisture measuring instrument has not been calibrated
Check calibration/ moisture standard
4. GLASS ADHESION /PENETRATION RESISTANCE
4.1 GLASS ADHESION /PENETRATION RESISTANCE Die Normally the measurements are carried out with the pummel or compression shear test.
Check origin of glass/coating/ glass treatment/storage conditions/Fire or tin side to the PVB (check with UV lamp)
Quality of glass washing
Check washing conditions/ degree of glass drying Washing water conductivity ≤ 20 µS, detergents?
Incorrect autoclave cycle
Check parameters, control instruments
Adhesion test (e.g. pummel temperature > -18°C/0°F)
Implementation acc. to instructions/ personnel training (Pummel test: -18°C/0°F)
Impurities on glass/on PVB
Cleanliness of lay-up room Cleanliness of glass/PVB
PVB film quality
Change film type Check with Technical Service TROSIFOL
Ball-drop test/ head form test not passed
Falling height too low/ glass adhesion too high
Carrying out the test acc. to instructions/standards. Number and thickness of the specimens Check PVB film thickness/after stretching Temperature of the glass samples incorrect (should be: 23°C/73°F)
5. LAMINATED SAFETY GLASS ONLY PARTLY OK
5.1 LAMINATED SAFETY GLASS ONLY PARTLY OK
Fault
Cause
Optimization
Laminated safety glass only partly ok after production process
Uneven temperature distribution in the autoclave
Check function of autoclave (fan, display instrument, etc.)
Laminated Safety Glass autoclaved in too thick layers (inner layer too cold)
Lengthen holding time
Pressure points with thinned film/diminished colour (with colour films) due to excessive clamping pressure of the glass in the autoclave
Change packing density Check degree of clamping
This glossary is available in German language only.